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Picture for Assessment of the Hydrogen Induced Stress Cracking Resistance of Precipitation Hardened Nickel-based Alloys using the Slow Strain Rate Tensile Test Method – Influence of Microstructure
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Assessment of the Hydrogen Induced Stress Cracking Resistance of Precipitation Hardened Nickel-based Alloys using the Slow Strain Rate Tensile Test Method – Influence of Microstructure

Product Number: 51319-13365-SG
Author: Ilaria Salvatori
Publication Date: 2019
$20.00

Within the framework of a Joint Industrial Project sponsored by several petroleum companies the behavior of several Precipitation Hardened (PH) Ni-based alloys with respect to Hydrogen Induced Stress Cracking (HISC) resistance was studied using the Slow Strain Rate Tensile (SSRT) test method conducted under hydrogen charging conditions (applying a constant cathodic current density throughout the test). Among the test materials several industrial heats of UNS N07718 UNS N09945/945X UNS N09925 UNS N07725 were evaluated.A detailed microstructural analysis was performed on each heat at different levels involving SEM-FEG examinations at high magnification on etched samples to reveal the phases present at grain boundaries. Methodologies were developed to quantify the grain boundary coverage (length of precipitates at grain boundary divided by the total grain boundary length) and to study the distribution in size (equivalent diameter surface shape factor) of the grain boundary precipitates and applied to the studied materials.Elemental chemical analysis of the precipitates was also conducted by Energy Dispersive Xray spectrometry. Systematic fracture surface examinations were performed after SSRT tests under hydrogen charging conditions and compared to those obtained after SSRT tests in an inert environment.The performance of the different alloys with respect to HISC resistance is discussed on the basis of the plastic elongation obtained in the SSRT tests under cathodic polarization the microstructural features the cracking mode and the microstructural criteria given in the API 6A CRA standard.

Picture for Atmospheric Corrosion Behaviour Of Zinc And Zinc Alloys: Comparison Between Natural And Accelerated Exposure
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Atmospheric Corrosion Behaviour Of Zinc And Zinc Alloys: Comparison Between Natural And Accelerated Exposure

Product Number: 51321-16804-SG
Author: Marco Ormellese; Silvia Beretta; Tiziano Bellezze; Fabio Bolzoni
Publication Date: 2021
$20.00
Picture for Atmospheric Corrosion Through the Eyes of a Computer Simulation
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Atmospheric Corrosion Through the Eyes of a Computer Simulation

Product Number: 51321-16394-SG
Author: Agnieszka Franczak/Leslie Bortels/Christophe Baeté /Bart Van den Bossche
Publication Date: 2021
$20.00
Picture for Avoid Potential Repeated Failure (Cracked Gas Compressor line) Through Proper Material Assessment
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Avoid Potential Repeated Failure (Cracked Gas Compressor line) Through Proper Material Assessment

Product Number: MPWT19-14239
Author: Ahmed Elsharkawi, Amro Hassanein
Publication Date: 2019
$0.00

The heat treatment condition of industrial materials is a critical parameter for material evaluation and its fitness for intended service. Proper heat treatment will produce desired mechanical and physical properties, while absence or improper heat treatment may lead to major failure with huge production, Environmental, Health, and Safety (EHS) impacts. We hereby explain an actual case for cracked gas compressor (CGC) 5th stage discharge line caustic stress corrosion cracking (SCC) that caused unplanned plant shut down and resulted in noticed financial and production loss.
The proven root cause is absence of normalization. Emergency piping batch is received and supposed to be normalized to avoid failure recurrence. Many discrepancies extracted from submitted material certificates, also many physical signs observed on the material itself raising doubts about received material compatibility. Using advanced Positive Material Identification (PMI) device to verify the chemical composition of the received material, results show that the material is questionable.
As a precise test to verify heat treatment condition, microstructure analysis test (metallography) conducted to confirm normalization condition of the material, the resulted grain structure size and growth confirm that one of the received pipes has improper or absence of normalization.
The material rejected as it is proven and confirmed that it is not normalized as per the requirements to avoid further potential of hydrocarbon leakage due to improper material specification. Rejecting the material eliminate the potential of having repeated failure, in addition to 600,000 Saudi Riyal (SR) cost saving as material cost. A common recommendation shared with concerned parties to consider metallography as a mandatory test to be submitted with heat-treated material test certificate (MTC).
Key words: Heat treatment, microstructure, normalization, grain structure, failure, metallography

Picture for Behaviour of Damaged Thermally Sprayed Aluminium (TSA) in Aerated and Deaerated Seawater
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Behaviour of Damaged Thermally Sprayed Aluminium (TSA) in Aerated and Deaerated Seawater

Product Number: 51319-12766-SG
Author: Shiladitya Paul
Publication Date: 2019
$20.00