Server maintenance is scheduled for Saturday, December 21st between 6am-10am CST.

During that time, parts of our website will be affected until maintenance is completed. Thank you for your patience.

Menu
Search
Filters
Close
Menu

Use GIVING24 at checkout to save 20% on eCourses and books (some exclusions apply)!

99151 APPLICATION OF ELECTROCHEMICAL IMPEDANCE SPECTROSCOPY (EIS) FOR MONITORING OF SCCCRACKS

Picture for 99151 APPLICATION OF ELECTROCHEMICAL IMPEDANCE
Available for download
Product Number: 51300-99151-SG
ISBN: 99151 1999 CP
Author: R.W. Bosch, F. Moons, J.H. Zheng and W.F. Bogaerts
$0.00
$20.00
$20.00
It was investigated if Electrochemical Impedance Spectroscopy (EIS) could be used for the monitoring of Stress Corrosion Cracking (SCC). First a model was developed that described the impedance response of a cracked surface, i.e. the model could distinguish between a flat electrode surface and a surface with cracks. Experiments with stainless steel electrodes with artificial “cracks” (electrically drilled small holes) in 0.1 M Na2SO4 showed that the influence of the artificial “cracks” on the impedance response was mainly reflected in the phase shift at frequencies between 100 and 1 Hz. To generate real stress corrosion cracks, Slow Strain Rate Tests (SSRT) were performed with sensitised SS 304 specimen in a 5 N H2SO4+ 0.1 M NaCl solution at room temperature. Analysis of the fi-acture surface clearly shows intergranular attack, suggesting that stress corrosion cracks were formed. Impedance measurements were performed tsvice an hour during experiments with stress (SSRT) and without stress. Phase shifts at frequencies 100 and 10 Hz showed a clear difference between the results with stress and without stress suggesting that stress corrosion cracks were detected by the impedance measurements. Keywords: Stress Corrosion Cracking, Electrochemical Impedance Spectroscopy,Slow Strain Rate Test, stainless steel
It was investigated if Electrochemical Impedance Spectroscopy (EIS) could be used for the monitoring of Stress Corrosion Cracking (SCC). First a model was developed that described the impedance response of a cracked surface, i.e. the model could distinguish between a flat electrode surface and a surface with cracks. Experiments with stainless steel electrodes with artificial “cracks” (electrically drilled small holes) in 0.1 M Na2SO4 showed that the influence of the artificial “cracks” on the impedance response was mainly reflected in the phase shift at frequencies between 100 and 1 Hz. To generate real stress corrosion cracks, Slow Strain Rate Tests (SSRT) were performed with sensitised SS 304 specimen in a 5 N H2SO4+ 0.1 M NaCl solution at room temperature. Analysis of the fi-acture surface clearly shows intergranular attack, suggesting that stress corrosion cracks were formed. Impedance measurements were performed tsvice an hour during experiments with stress (SSRT) and without stress. Phase shifts at frequencies 100 and 10 Hz showed a clear difference between the results with stress and without stress suggesting that stress corrosion cracks were detected by the impedance measurements. Keywords: Stress Corrosion Cracking, Electrochemical Impedance Spectroscopy,Slow Strain Rate Test, stainless steel
PRICE BREAKS - The more you buy, the more you save
Quantity
1+
5+
Price
$20.00
$20.00
Product tags
Also Purchased
Picture for 99153 THE CORRELATION BETWEEN CRACK CHEMISTRY
Available for download

99153 THE CORRELATION BETWEEN CRACK CHEMISTRY AND CRACK GROWTH BEHAVIOR OF 7XXX SERIES ALUMINUM ALLOYS: A COMPARISON OF FIELD AND LABORATORY TESTS

Product Number: 51300-99153-SG
ISBN: 99153 1999 CP
Author: K.R. Cooper, R.G. Kelly, E. L. Colvin
$20.00
Picture for 99152 Intergranular Cracking in High-Strength,
Available for download

99152 Intergranular Cracking in High-Strength, Cold-Rolled, and Precipitation-Hardened Austenitic Stainless Steel UNS S35500

Product Number: 51300-99152-SG
ISBN: 99152 1999 CP
Author: Sharad P. Pednekar, Victor K. Champagne, Marc S. Pepi, and Scott Grendahl
$20.00
Picture for 99154 HYDRIDE FORMATION AND GROWTH IN
Available for download

99154 HYDRIDE FORMATION AND GROWTH IN GRADE 2 TITANIUM IN 3,5%NACL SOLUTION

Product Number: 51300-99154-SG
ISBN: 99154 1999 CP
Author: Z, F. Wang, C. L. Briant, K. S. Kurnar and N. Chollacoop
$20.00
Categories
Industry
Recently viewed
Popular tags
View all

Association for Materials Protection and Performance

© AMPP All Rights Reserved.
Membership Terms of Content Use
Contact Customer Support